Structural Analysis for the Single Crystal of 2-(4-(9H-carbazol-9-yl)benzylidene) based Dye Compound

황지용; Young-A Son (손영아)

Structural Analysis for the Single Crystal of 2-(4-(9H-carbazol-9-yl)benzylidene) based Dye Compound

Textile Coloration and Finishing
Abbr : Text. Color. and Finish.
2014, 26(2), pp.143-149
Publisher : The Korean Society Of Dyers And Finishers
Research Area : Engineering > Fiber Engineering > Dyeing Engineering

황지용 ¹, Young-A Son ¹

¹충남대학교

Accredited

ABSTRACT

The designed dye material, namely 2-(4-(9H-carbazol-9-yl)benzylidene) compound, was synthesized. After the reaction, the solid was filtered and purified by recrystalization with acetone/water. To confirm and analyze its synthesis and structural formation, the single crystal was prepared and its measurement was carried out. A yellow needle crystal of C22H13N3 were made on a Rigaku R-AXIS RAPID diffractometer using graphite monochromated CuKα radiation. All details were suggested and introduced to support and communicate this study.

KEYWORDS

carbazol, benzylidene, malononitrile, C22H13N3, orthorhombic, single crystal

Citation status

* References for papers published after 2023 are currently being built.

[journal] X. Li / 2009 / Optical Properties of Donor-π-(accepter)n Merocyanine Dyes with Dicyanovinylindane as Acepter Group and Triphenylamine as Donor Unit / Dyes and Pigments 82 : 293~

[other] S. Horie / 1984 / Electrophorographic Light-sensitive Materials, United States Patent, US 4469678 /

[other] M. Murakami / 1996 / Electroluminescent Device Containing Anthraquinone Derivative or Indandione Derivative / Japanese Kokai Tokkyo Koho JP 08097465

[other] E. Kato / 2004 / Cellulose Acylate Films, their Manufacture, Optical Films, Liguid-crystal Displays, and Silver Halide Photographic Materials / Japanese Kokai Tokkyo Koho, JP 2004042381

[other] / 2000 / Crystal Structure Analysis Package / Crystal Structure 4. 0, Rigaku Corporation : 196~8666

[journal] M. C. Burla / 2005 / An Improved Tool for Crystal Structure Determination and Refinement / J. of Applied Crystallography 38 : 381~

[journal] G. M. Sheldrick / 2008 / A Short History of SHELX / Acta Crystallographica Section A 64 : 112~

[journal] V. V. Nesterov / 2007 / Search for New Potential NLO Crystalline Materials: Chiral Derivatives of (2S)-2-(methoxymethyl)pyrrolidine / J. of Molecular Structure 831 : 18~

[other] / 1998 / Crystal Structure Analysis Package / Crystal Structure 3.8, Rigaku and Rigaku/MSC

[journal] A. Altomare / 1994 / A Program for Automatic Solution of Crystal Structures by Direct Methods optimized for Powder Data / J. of Applied Crystallography 27 : 435~

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