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Microwave-assisted one-pot synthesis of iron(II, III) oxide/reduced graphene oxide for an application of supercapacitor electrode

  • Carbon Letters
  • Abbr : Carbon Lett.
  • 2019, 29(4), pp.411-418
  • DOI : 10.1007/s42823-019-00045-9
  • Publisher : Korean Carbon Society
  • Research Area : Natural Science > Natural Science General > Other Natural Sciences General
  • Received : October 15, 2018
  • Accepted : June 17, 2019
  • Published : August 1, 2019

KIM JEONGHYUN 1 Jung Yongju ORD ID 2 Kim Seok 1

1부산대학교
2한국기술교육대학교

Accredited

ABSTRACT

Graphene and Fe3O4 were bound by electrostatic attraction and prepared by effective reduction through microwave treatments. As a result of fabricating graphene with Fe3O4 as a composite material, it has been confirmed that it contributes to the structural improvement in graphene stabilization and at the same time, it shows improved electrochemical performance through improved charge transfer. It was also confirmed that the crystalline Fe3O4 was uniformly dispersed in the rGO sheet, effectively blocking the reaggregation due to the van der Waals interaction between the neighboring rGO sheets. The structural analysis of prepared composites was confirmed by transmission electron microscopy, and X-ray diffractometer. Electrochemical properties of composites were studied by cyclic voltammetry, galvanostatic charge–discharge curves, and electrochemical impedance spectroscopy. The Fe3O4 (0.4 M)/rGO composite showed a high specific capacitance of 972 F g−1 at the current density of 1 A g−1 in 6 M KOH electrolyte, which is higher than that of the pristine materials rGO (251 F g−1) and Fe3O4 (183 F g−1). Also, the prepared composites showed a very stable cyclic behavior at high current density, as well as an improvement in comparison with pristine materials in terms of resistance.

Citation status

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Total Citation Counts(KCI+WOS) (10) This is the number of times that the duplicate count has been removed by comparing the citation list of WoS and KCI.

Scopus Citation Counts (12) This is the result of checking the information with the same ISSN, publication year, volume, and start page between articles in KCI and the SCOPUS journals. (as of 2024-10-01)

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