@article{ART003273353},
author={Mohammad Khazaei Nejad and Hassan Ali Zamani},
title={Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents},
journal={Carbon Letters},
issn={1976-4251},
year={2025},
volume={35},
number={4},
pages={1667-1675},
doi={10.1007/s42823-025-00882-x}
TY - JOUR
AU - Mohammad Khazaei Nejad
AU - Hassan Ali Zamani
TI - Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents
JO - Carbon Letters
PY - 2025
VL - 35
IS - 4
PB - Korean Carbon Society
SP - 1667
EP - 1675
SN - 1976-4251
AB - This research developed a highly efficient voltammetric sensor, utilizing a carbon paste electrode (CPE) integrated with a novel ZnO-doped Pd–Pt bimetallic catalyst decorated with reduced graphene oxide (ZnO-Pt@Pd/rGO) and 1-ethyl-3-methylimidazolium bis(trifluoromethanesulfonyl)imide ([EMIM][Tf2N]), for the precise determination of sulfafurazole in real dextrose saline and tablet samples. The ZnO-Pt@Pd/rGO nanocomposite was synthesized through a one-stage synthesis process and characterized using SEM and EDS techniques. The comparison of the ZnO-Pt@Pd/rGO/[EMIM][Tf2N]/CPE with unmodified CPE, ZnO-Pt@Pd/rGO/CPE, and [EMIM][Tf2N]/CPE confirms the synergic effect of ZnO-Pt@Pd/rGO and [EMIM][Tf2N] as two conductive catalysts in fabrication of new sensor. The resulting sensor exhibited remarkable stability over a period of 2 months without compromising its efficiency for sulfafurazole detection. With a linear range of 0.001–250 µM (R2 = 0.9971) and LOD of 0.4 nM, ZnO-Pt@Pd/rGO/[EMIM][Tf2N]/CPE showcased exceptional accuracy and precision in the monitoring of sulfafurazole. Validation using real tablet and dextrose saline samples confirmed the sensor's outstanding capability in determining sulfafurazole, with relative recoveries ranging from 98.92 to 103.8% offering a promising solution for reliable sulfafurazole analysis in diverse pharmaceutical samples.
KW - Sulfafurazole;Pharmaceutical analysis;Voltammetric sensor;Carbon-based catalyst
DO - 10.1007/s42823-025-00882-x
ER -
Mohammad Khazaei Nejad and Hassan Ali Zamani. (2025). Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents. Carbon Letters, 35(4), 1667-1675.
Mohammad Khazaei Nejad and Hassan Ali Zamani. 2025, "Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents", Carbon Letters, vol.35, no.4 pp.1667-1675. Available from: doi:10.1007/s42823-025-00882-x
Mohammad Khazaei Nejad, Hassan Ali Zamani "Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents" Carbon Letters 35.4 pp.1667-1675 (2025) : 1667.
Mohammad Khazaei Nejad, Hassan Ali Zamani. Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents. 2025; 35(4), 1667-1675. Available from: doi:10.1007/s42823-025-00882-x
Mohammad Khazaei Nejad and Hassan Ali Zamani. "Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents" Carbon Letters 35, no.4 (2025) : 1667-1675.doi: 10.1007/s42823-025-00882-x
Mohammad Khazaei Nejad; Hassan Ali Zamani. Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents. Carbon Letters, 35(4), 1667-1675. doi: 10.1007/s42823-025-00882-x
Mohammad Khazaei Nejad; Hassan Ali Zamani. Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents. Carbon Letters. 2025; 35(4) 1667-1675. doi: 10.1007/s42823-025-00882-x
Mohammad Khazaei Nejad, Hassan Ali Zamani. Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents. 2025; 35(4), 1667-1675. Available from: doi:10.1007/s42823-025-00882-x
Mohammad Khazaei Nejad and Hassan Ali Zamani. "Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents" Carbon Letters 35, no.4 (2025) : 1667-1675.doi: 10.1007/s42823-025-00882-x