@article{ART003273353},
author={Nejad Mohammad Khazaei and Zamani Hassan Ali},
title={Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents},
journal={Carbon Letters},
issn={1976-4251},
year={2025},
volume={35},
number={4},
pages={1667-1675},
doi={10.1007/s42823-025-00882-x}
TY - JOUR
AU - Nejad Mohammad Khazaei
AU - Zamani Hassan Ali
TI - Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents
JO - Carbon Letters
PY - 2025
VL - 35
IS - 4
PB - Korean Carbon Society
SP - 1667
EP - 1675
SN - 1976-4251
AB - This research developed a highly efficient voltammetric sensor, utilizing a carbon paste electrode (CPE) integrated with a novel ZnO-doped Pd–Pt bimetallic catalyst decorated with reduced graphene oxide (ZnO-Pt@Pd/rGO) and 1-ethyl-3-methylimidazolium bis(trifluoromethanesulfonyl)imide ([EMIM][Tf2N]), for the precise determination of sulfafurazole in real dextrose saline and tablet samples. The ZnO-Pt@Pd/rGO nanocomposite was synthesized through a one-stage synthesis process and characterized using SEM and EDS techniques. The comparison of the ZnO-Pt@Pd/rGO/[EMIM][Tf2N]/CPE with unmodified CPE, ZnO-Pt@Pd/rGO/CPE, and [EMIM][Tf2N]/CPE confirms the synergic effect of ZnO-Pt@Pd/rGO and [EMIM][Tf2N] as two conductive catalysts in fabrication of new sensor. The resulting sensor exhibited remarkable stability over a period of 2 months without compromising its efficiency for sulfafurazole detection. With a linear range of 0.001–250 µM (R2 = 0.9971) and LOD of 0.4 nM, ZnO-Pt@Pd/rGO/[EMIM][Tf2N]/CPE showcased exceptional accuracy and precision in the monitoring of sulfafurazole. Validation using real tablet and dextrose saline samples confirmed the sensor's outstanding capability in determining sulfafurazole, with relative recoveries ranging from 98.92 to 103.8% offering a promising solution for reliable sulfafurazole analysis in diverse pharmaceutical samples.
KW - Sulfafurazole;Pharmaceutical analysis;Voltammetric sensor;Carbon-based catalyst
DO - 10.1007/s42823-025-00882-x
ER -
Nejad Mohammad Khazaei and Zamani Hassan Ali. (2025). Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents. Carbon Letters, 35(4), 1667-1675.
Nejad Mohammad Khazaei and Zamani Hassan Ali. 2025, "Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents", Carbon Letters, vol.35, no.4 pp.1667-1675. Available from: doi:10.1007/s42823-025-00882-x
Nejad Mohammad Khazaei, Zamani Hassan Ali "Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents" Carbon Letters 35.4 pp.1667-1675 (2025) : 1667.
Nejad Mohammad Khazaei, Zamani Hassan Ali. Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents. 2025; 35(4), 1667-1675. Available from: doi:10.1007/s42823-025-00882-x
Nejad Mohammad Khazaei and Zamani Hassan Ali. "Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents" Carbon Letters 35, no.4 (2025) : 1667-1675.doi: 10.1007/s42823-025-00882-x
Nejad Mohammad Khazaei; Zamani Hassan Ali. Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents. Carbon Letters, 35(4), 1667-1675. doi: 10.1007/s42823-025-00882-x
Nejad Mohammad Khazaei; Zamani Hassan Ali. Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents. Carbon Letters. 2025; 35(4) 1667-1675. doi: 10.1007/s42823-025-00882-x
Nejad Mohammad Khazaei, Zamani Hassan Ali. Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents. 2025; 35(4), 1667-1675. Available from: doi:10.1007/s42823-025-00882-x
Nejad Mohammad Khazaei and Zamani Hassan Ali. "Development of a graphene-based bimetallic catalyst for enhanced voltammetric detection of sulfafurazole antimicrobial agents" Carbon Letters 35, no.4 (2025) : 1667-1675.doi: 10.1007/s42823-025-00882-x