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Fabrication of TiNx by planetary milling

  • Journal of the Korean Crystal Growth and Crystal Technology
  • Abbr : J. Korean Cryst. Growth Cryst. Technol.
  • 2005, 15(3), pp.104-107
  • Publisher : The Korea Association Of Crystal Growth, Inc.
  • Research Area : Engineering > Materials Science and Engineering

Sungjin Kim 1 김동식 1 라노 1 Sungbum Park 2 권원일 1 김문협 1 Heung-Sik Woo 3 Jung-Ho Ahn 4

1금오공과대학교
2
3동국대학교
4안동대학교

Accredited

ABSTRACT

TiNx powder have been fabrication by making of reaction between titanium powder and Si3N4 bowl during a planetary milling. Milling times were maintained for 1hour, 5hours, and 10hours, respectively. The XRD result showed existence of non-stoichiometric compound of TiN0.26 after 5hours milling and coexistence of TiN with TiN0.26 after 10hours milling. Particle size distribution was investigated by particle size analyzer and microstructure was analyzed by FE-SEM. The size of titanium was decreased with increasing the milling time and the mean size of TiNx after 10hours milling was increased by 200nm.

Citation status

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