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SiC powders synthesized from rice husk

  • Journal of the Korean Crystal Growth and Crystal Technology
  • Abbr : J. Korean Cryst. Growth Cryst. Technol.
  • 2016, 26(5), pp.188-192
  • DOI : 10.6111/JKCGCT.2016.26.5.188
  • Publisher : The Korea Association Of Crystal Growth, Inc.
  • Research Area : Engineering > Materials Science and Engineering
  • Received : March 31, 2016
  • Accepted : September 23, 2016
  • Published : October 31, 2016

Tae-Eon Park 1 Jun Yeon Hwang 2 Jin Seong Lim 2 Young-Hoon Yun 3

1(주)에코텍코리아
2한국과학기술원 전북분원
3동신대학교

Accredited

ABSTRACT

In this work, the SiC powders were synthesized through the carbonized matter from the mixture of silica powder and rice husks. The SiC powders, obtained from the carbothermal reduction reaction of silica and carbonized rice husks, were investigated by XRD patterns, XPS, FE-SEM and FE-TEM. In the XRD patterns, the specimens showed clearly very high strong peak of (111) plane near 35 o as well as weak (220) and (311) peak respectively at approximately 60 o and 72 o . Under Ar atmosphere, the power synthesized from the mixture (in case of mixing ratio, 6 : 4) of carbonized rice husks and silica showed mainly cubic SiC crystalline phase showing relatively lower ratio of hexagonal phase without residual carbon in XRD pattern. In the TEM analysis, the specimen, synthesized from carbonized rice husks and silica with mixing ratio of 6 : 4 under Ar atmosphere, showed relatively fine particles under 5 μm and a crystalline SiC phase of (100) diffraction pattern.

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