@article{ART002746851},
author={LEEJAEYEON and Yong Jin Kim and Dae Sung Kim and Hyosoon Shin and Nahm, Sahn and Myoungpyo Chun},
title={Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures},
journal={Journal of the Korean Crystal Growth and Crystal Technology},
issn={1225-1429},
year={2021},
volume={31},
number={4},
pages={166-173},
doi={10.6111/JKCGCT.2021.31.4.166}
TY - JOUR
AU - LEEJAEYEON
AU - Yong Jin Kim
AU - Dae Sung Kim
AU - Hyosoon Shin
AU - Nahm, Sahn
AU - Myoungpyo Chun
TI - Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures
JO - Journal of the Korean Crystal Growth and Crystal Technology
PY - 2021
VL - 31
IS - 4
PB - The Korea Association Of Crystal Growth, Inc.
SP - 166
EP - 173
SN - 1225-1429
AB - The rutile phase of TiO2 forms a stable phase at high temperatures compared to anatase phase, but the stable temperature range of anatase changes depending on the synthesis conditions. In this study, nano-sized TiO2 was synthesized by the Sol-gel method using TiOSO4 and a mixed solvent of ethanol and distilled water, and the phase change of anatase and rutile according to pH and heat treatment temperature was investigated. Changes in the ratio of anatase and rutile wereobserved by changing the pH (3, 5, 7, 9) and heat treatment temperature (500, 600, 700, 800, 900°C) conditions of the prepared TiO2. As a result of observing these changes through XRD and FE-SEM analysis, anatase TiO2 at 500°C and rutile TiO2 at 900°C were observed. According to the pH, at these intermediate temperatures of 600, 700 and 800°C, the ratio of anatase and rutile changes. At 700°C, it was concluded that pH = 3~5 had a larger ratio of anatase TiO2, andpH = 7~9 had a larger ratio of rutile TiO2.
KW - TiO2;Rutile;Anatase;Synthesis;XRD;Crystallite size
DO - 10.6111/JKCGCT.2021.31.4.166
ER -
LEEJAEYEON, Yong Jin Kim, Dae Sung Kim, Hyosoon Shin, Nahm, Sahn and Myoungpyo Chun. (2021). Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures. Journal of the Korean Crystal Growth and Crystal Technology, 31(4), 166-173.
LEEJAEYEON, Yong Jin Kim, Dae Sung Kim, Hyosoon Shin, Nahm, Sahn and Myoungpyo Chun. 2021, "Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures", Journal of the Korean Crystal Growth and Crystal Technology, vol.31, no.4 pp.166-173. Available from: doi:10.6111/JKCGCT.2021.31.4.166
LEEJAEYEON, Yong Jin Kim, Dae Sung Kim, Hyosoon Shin, Nahm, Sahn, Myoungpyo Chun "Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures" Journal of the Korean Crystal Growth and Crystal Technology 31.4 pp.166-173 (2021) : 166.
LEEJAEYEON, Yong Jin Kim, Dae Sung Kim, Hyosoon Shin, Nahm, Sahn, Myoungpyo Chun. Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures. 2021; 31(4), 166-173. Available from: doi:10.6111/JKCGCT.2021.31.4.166
LEEJAEYEON, Yong Jin Kim, Dae Sung Kim, Hyosoon Shin, Nahm, Sahn and Myoungpyo Chun. "Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures" Journal of the Korean Crystal Growth and Crystal Technology 31, no.4 (2021) : 166-173.doi: 10.6111/JKCGCT.2021.31.4.166
LEEJAEYEON; Yong Jin Kim; Dae Sung Kim; Hyosoon Shin; Nahm, Sahn; Myoungpyo Chun. Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures. Journal of the Korean Crystal Growth and Crystal Technology, 31(4), 166-173. doi: 10.6111/JKCGCT.2021.31.4.166
LEEJAEYEON; Yong Jin Kim; Dae Sung Kim; Hyosoon Shin; Nahm, Sahn; Myoungpyo Chun. Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures. Journal of the Korean Crystal Growth and Crystal Technology. 2021; 31(4) 166-173. doi: 10.6111/JKCGCT.2021.31.4.166
LEEJAEYEON, Yong Jin Kim, Dae Sung Kim, Hyosoon Shin, Nahm, Sahn, Myoungpyo Chun. Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures. 2021; 31(4), 166-173. Available from: doi:10.6111/JKCGCT.2021.31.4.166
LEEJAEYEON, Yong Jin Kim, Dae Sung Kim, Hyosoon Shin, Nahm, Sahn and Myoungpyo Chun. "Phase stability of TiO2 synthesized by Sol-gel Method at various pH and calcination temperatures" Journal of the Korean Crystal Growth and Crystal Technology 31, no.4 (2021) : 166-173.doi: 10.6111/JKCGCT.2021.31.4.166
