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Electroanalysis of nirofurazone at silver particles and graphite powder composite electrode

  • Carbon Letters
  • Abbr : Carbon Lett.
  • 2022, 32(3), pp.767-780
  • DOI : 10.1007/s42823-021-00307-5
  • Publisher : Korean Carbon Society
  • Research Area : Natural Science > Natural Science General > Other Natural Sciences General
  • Received : September 13, 2021
  • Accepted : November 11, 2021
  • Published : May 1, 2022

Zoubir J. 1 Assabbane A. 1 Bakas I. 1

1Team of Catalysis and Environment Ibn Zohr University Faculty of Sciences, BP 8106, Agadir, Morocco

Accredited

ABSTRACT

The main objective of the research was to deposit thin films of silver on a graphite carbon paste in a phosphate buffer medium using an electrochemical method. To construct a nitrofurazone detection sensor that is highly sensitive. Different manufacturing parameters, such as electrodeposition potential, pH effect, potential scan rate effect, and number of scan cycles, were examined in this section. The parameters were optimized to improve the deposited silver layers various electrocatalytic characteristics. The Nitrofurazone reduction process is diffusion controlled, as seen by the linear variation of Epc with log(v). The constructed Ag-NPs@CPE electrod has excellent electrical characteristics a large active surface area and low background with extremely high electrical conductivity, according to structural and electrochemical characterizations such as Scanning electron microscopy, X-ray diffraction (XRD) and cyclic voltammetry. The constructed sensor has a very remarkable analytical performance for nitrofurazone molecule identification, with a very low detection limit of about 10–8 M. The detection of nitrofurazone using our Ag-NPs@CPE sensors in real samples contaminated with the antibiotic nitrofurazone, such as tap water and urine. In the selected sample, the electroanalytical findings reveal a very satisfactory recovery rate of more than 94 percent.

Citation status

This is the result of checking the information with the same ISSN, publication year, volume, and start page between the WoS and the KCI journals. (as of 2023-07-13)

Total Citation Counts(KCI+WOS) (7) This is the number of times that the duplicate count has been removed by comparing the citation list of WoS and KCI.

Scopus Citation Counts (7) This is the result of checking the information with the same ISSN, publication year, volume, and start page between articles in KCI and the SCOPUS journals. (as of 2023-10-01)

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