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Influence of graphite platelets with and without SiC on the densification and fracture toughness of ZrB2 ceramic sintered by SPS

  • Carbon Letters
  • Abbr : Carbon Lett.
  • 2022, 32(6), pp.1559-1566
  • DOI : 10.1007/s42823-022-00389-9
  • Publisher : Korean Carbon Society
  • Research Area : Natural Science > Natural Science General > Other Natural Sciences General
  • Received : June 8, 2022
  • Accepted : August 10, 2022
  • Published : October 1, 2022

Savari Valid 1 Balak Zohre 1 Shahedifar Vahideh 2

1이란 아바즈 이슬람 아자드 대학 아바즈 분과 재료공학과
2이란 우르미아 소재 우르미아 대학교 공학부 재료공학과

Accredited

ABSTRACT

Few studies have been performed on ZrB2-graphite platelet composite made by spark plasma sintering (SPS) technique. In this research, the influence of adding graphite platelets (Gp) with and without SiC on the fracture toughness of ZrB2 ceramic was studied. The ZrB2-10Gp, ZrB2-15Gp, ZrB2-30SiC-10Gp, and ZrB2-30SiC-15Gp specimens were sintered by the SPS method at the temperature of 1850 °C for 8 min. The fracture toughness and work of fracture (WOF) were evaluated using the Single-Edge Notched Beam (SENB) technique. It was found that the fracture toughness and WOF were improved by the alone and combined addition of Gp and SiC to the monolithic ZrB2. The maximum fracture toughness of 4.8 ± 0.1 MPa m1/2 was obtained for the ZrB2-15Gp specimen. It seems that adding Gp alone was more effective in enhancing the fracture toughness of ZrB2 than the combined addition of Gp and SiC. While the addition of Gp and SiC simultaneously modified the densification behavior to reach full-densified samples.

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