@article{ART002964076},
author={Phuc Nguyen Thien and Giang Nguyen Thi Huong and An Vu Nguyen Thien Truong and Nam Nguyen Thanh Hoai and Anh Ly Duc and Nguyen Huynh Cam and An Hoang and Phong Mai Thanh and Hieu Nguyen Huu},
title={Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation},
journal={Carbon Letters},
issn={1976-4251},
year={2023},
volume={33},
number={2},
pages={489-500},
doi={10.1007/s42823-022-00439-2}
TY - JOUR
AU - Phuc Nguyen Thien
AU - Giang Nguyen Thi Huong
AU - An Vu Nguyen Thien Truong
AU - Nam Nguyen Thanh Hoai
AU - Anh Ly Duc
AU - Nguyen Huynh Cam
AU - An Hoang
AU - Phong Mai Thanh
AU - Hieu Nguyen Huu
TI - Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation
JO - Carbon Letters
PY - 2023
VL - 33
IS - 2
PB - Korean Carbon Society
SP - 489
EP - 500
SN - 1976-4251
AB - In this study, graphene oxide (GO) was synthesized by the improved Hummers’ method. The degree of oxidation from graphite (Gi) to GO was determined through interlayer spacing calculated from X–ray diffraction. Besides, the effect of KMnO4:Gi ratios (X1), H2SO4 volume (X2), oxidation temperature (X3), oxidation time of stage 1 (X4), and oxidation time of stage 2 (X5) was screened by the Plackett–Burman model. The simultaneous impact of three factors that influenced the degree of oxidation (X1, X2, and X3) was studied by the Box–Behnken experimental model of response surface methodology to achieve suitable conditions for the GO synthesis process. The characterization of GO product was investigated via the modern analytical methods: X-ray diffraction, Raman spectroscopy, Fourier transform infrared spectroscopy, UV–Vis spectroscopy, field emission scanning electron microscopy, transmission electron microscopy, and atomic force microscopy. In addition, the study was also carried out on a pilot scale for orientation in industrial application with the yield of 14 g/batch.
KW - Graphene oxide Synthesis procedures Degree of oxidation
DO - 10.1007/s42823-022-00439-2
ER -
Phuc Nguyen Thien, Giang Nguyen Thi Huong, An Vu Nguyen Thien Truong, Nam Nguyen Thanh Hoai, Anh Ly Duc, Nguyen Huynh Cam, An Hoang, Phong Mai Thanh and Hieu Nguyen Huu. (2023). Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation. Carbon Letters, 33(2), 489-500.
Phuc Nguyen Thien, Giang Nguyen Thi Huong, An Vu Nguyen Thien Truong, Nam Nguyen Thanh Hoai, Anh Ly Duc, Nguyen Huynh Cam, An Hoang, Phong Mai Thanh and Hieu Nguyen Huu. 2023, "Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation", Carbon Letters, vol.33, no.2 pp.489-500. Available from: doi:10.1007/s42823-022-00439-2
Phuc Nguyen Thien, Giang Nguyen Thi Huong, An Vu Nguyen Thien Truong, Nam Nguyen Thanh Hoai, Anh Ly Duc, Nguyen Huynh Cam, An Hoang, Phong Mai Thanh, Hieu Nguyen Huu "Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation" Carbon Letters 33.2 pp.489-500 (2023) : 489.
Phuc Nguyen Thien, Giang Nguyen Thi Huong, An Vu Nguyen Thien Truong, Nam Nguyen Thanh Hoai, Anh Ly Duc, Nguyen Huynh Cam, An Hoang, Phong Mai Thanh, Hieu Nguyen Huu. Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation. 2023; 33(2), 489-500. Available from: doi:10.1007/s42823-022-00439-2
Phuc Nguyen Thien, Giang Nguyen Thi Huong, An Vu Nguyen Thien Truong, Nam Nguyen Thanh Hoai, Anh Ly Duc, Nguyen Huynh Cam, An Hoang, Phong Mai Thanh and Hieu Nguyen Huu. "Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation" Carbon Letters 33, no.2 (2023) : 489-500.doi: 10.1007/s42823-022-00439-2
Phuc Nguyen Thien; Giang Nguyen Thi Huong; An Vu Nguyen Thien Truong; Nam Nguyen Thanh Hoai; Anh Ly Duc; Nguyen Huynh Cam; An Hoang; Phong Mai Thanh; Hieu Nguyen Huu. Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation. Carbon Letters, 33(2), 489-500. doi: 10.1007/s42823-022-00439-2
Phuc Nguyen Thien; Giang Nguyen Thi Huong; An Vu Nguyen Thien Truong; Nam Nguyen Thanh Hoai; Anh Ly Duc; Nguyen Huynh Cam; An Hoang; Phong Mai Thanh; Hieu Nguyen Huu. Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation. Carbon Letters. 2023; 33(2) 489-500. doi: 10.1007/s42823-022-00439-2
Phuc Nguyen Thien, Giang Nguyen Thi Huong, An Vu Nguyen Thien Truong, Nam Nguyen Thanh Hoai, Anh Ly Duc, Nguyen Huynh Cam, An Hoang, Phong Mai Thanh, Hieu Nguyen Huu. Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation. 2023; 33(2), 489-500. Available from: doi:10.1007/s42823-022-00439-2
Phuc Nguyen Thien, Giang Nguyen Thi Huong, An Vu Nguyen Thien Truong, Nam Nguyen Thanh Hoai, Anh Ly Duc, Nguyen Huynh Cam, An Hoang, Phong Mai Thanh and Hieu Nguyen Huu. "Optimization of the eco-friendly synthesis of graphene oxide from graphite using Plackett–Burman and Box–Behnken models for industrial production orientation" Carbon Letters 33, no.2 (2023) : 489-500.doi: 10.1007/s42823-022-00439-2
