Influence of modified perylene-3, 4, 9, 10-tetracarboxylate with alkali metals ions as surfactant on the yield of hydrothermal liquid-phase exfoliated graphene sheets

Ahmad Nurin Jazlina; Mohamed Ruziana; Malek Mohd Firdaus; Sanusi Saedah Munirah; Muhamad Myzatul Azlyin; Ismail Ahmad Syakirin; Mahmood Mohamad Rusop

doi:10.1007/s42823-022-00442-7

Influence of modified perylene-3, 4, 9, 10-tetracarboxylate with alkali metals ions as surfactant on the yield of hydrothermal liquid-phase exfoliated graphene sheets

Carbon Letters
Abbr : Carbon Lett.
2023, 33(2), pp.531-548
DOI : 10.1007/s42823-022-00442-7
Publisher : Korean Carbon Society
Research Area : Natural Science > Natural Science General > Other Natural Sciences General
Received : August 7, 2022
Accepted : December 7, 2022
Published : March 1, 2023

Ahmad Nurin Jazlina ¹, Mohamed Ruziana ¹, Malek Mohd Firdaus ¹, Sanusi Saedah Munirah ¹, Muhamad Myzatul Azlyin ¹, Ismail Ahmad Syakirin ², Mahmood Mohamad Rusop ³

¹Faculty of Applied Sciences, Universiti Teknologi MARA
²MIMOS Semiconductor Sdn Bhd, Technology Park Malaysia
³NANO-SciTech Lab (NST), Centre for Functional Materials and Nanotechnology (FMN), Institute of Science (IOS), Universiti Teknologi MARA

Accredited

ABSTRACT

Combination of liquid-phase exfoliation and hydrothermal method has progressed in recent years mainly on production of 2D materials. In this study, graphene was successfully synthesized via combinatorial of liquid-phase exfoliation and hydrothermal method with the aid of various conductive surfactants perylene-3, 4, 9, 10-tetracarboxylate (PTCA), lithium perylene-3, 4, 9, 10-tetracarboxylate (LiPTCA) and sodium perylene-3, 4, 9, 10-tetracarboxylate (NaPTCA). The effect of the lithium (Li+) and sodium (Na+) cations toward the efficiency of the graphene exfoliation process and its electrical properties was thoroughly investigated. Based on the characterization techniques, it is revealed that NaPTCA is the ideal conductive surfactant to exfoliate graphene sheets. X-ray diffraction spectra verified that the Na+ cation certainly can enhance the exfoliation process by expanding the interlayer spacing. The lateral size of the graphene sheets with Na-PTCA surfactant was the smallest (4.17 µm) as observed from SEM micrograph. The maximum concentration of the graphene yield was achieved up to 0.151 mgmL−1 in NaPTCA surfactant alongside with excellent electrical conductivity of 746.27 Sm−1 and relevant specific capacitance of 129 Fg−1.

KEYWORDS

2D materials Graphene Hydrothermal Liquid-phase exfoliation Surfactant

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Carbon Letters 2023 KCI Impact Factor : 1.35 KCI-WoS Impact Factor : 6.04

Influence of modified perylene-3, 4, 9, 10-tetracarboxylate with alkali metals ions as surfactant on the yield of hydrothermal liquid-phase exfoliated graphene sheets

ABSTRACT

KEYWORDS

Citation status

This is the result of checking the information with the same ISSN, publication year, volume, and start page between the WoS and the KCI journals. (as of 2024-07-26)

Total Citation Counts(KCI+WOS) (1) This is the number of times that the duplicate count has been removed by comparing the citation list of WoS and KCI.

Scopus Citation Counts (2) This is the result of checking the information with the same ISSN, publication year, volume, and start page between articles in KCI and the SCOPUS journals. (as of 2024-10-01)

* References for papers published after 2023 are currently being built.

Carbon Letters 2023 KCI Impact Factor : 1.35 KCI-WoS Impact Factor : 6.04

Influence of modified perylene-3, 4, 9, 10-tetracarboxylate with alkali metals ions as surfactant on the yield of hydrothermal liquid-phase exfoliated graphene sheets

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Total Citation Counts(KCI+WOS) (1) This is the number of times that the duplicate count has been removed by comparing the citation list of WoS and KCI.

Scopus Citation Counts (2) This is the result of checking the information with the same ISSN, publication year, volume, and start page between articles in KCI and the SCOPUS journals. (as of 2024-10-01)

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