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Effect of the processing variables on the formation of Pb(Sc1/2Nb1/2)O3 thin layers

  • Journal of the Korean Crystal Growth and Crystal Technology
  • Abbr : J. Korean Cryst. Growth Cryst. Technol.
  • 2009, 19(2), pp.70~74
  • Publisher : The Korea Association Of Crystal Growth, Inc.
  • Research Area : Engineering > Materials Science and Engineering

Kyung Bong Park 1,  권승협 1,  Tae Heui Kim 1

1안동대학교

Accredited

ABSTRACT

Effect of the processing variables on the formation of Pb(Sc1/2Nb1/2)O3 (hereafter PSN) thin layers prepared on Pt(111)/Ti/SiO2/Si substrates using the sol-gel and the spin coating method has been studied. After each deposition, the coated films were heated at 370oC for 5 min. Then they were finally sintered at temperature range of 600~700oC by RTA(rapid thermal annealing). The final multilayered films showed a (111) preferred orientation. On a while, the layer-bylayer crystallization of multilayered amorphous thin films without the intermediate heating exhibited a (100) preferred orientation. In case of heat treatment in the tube furnace with the heating rate of 4oC/min, (100) and (111) oriented thin layers were formed simultaneously. The microstructure of the deposited films were dense and crack-free with thickness of 300nm, irrespective of the processing variables.

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