@article{ART000912029},
author={Sang Guen Lee and Eun Young Choi and Lee, Yoon-bok and KwangHo Kim and Park,Hee-Chan},
title={Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors},
journal={Journal of the Korean Crystal Growth and Crystal Technology},
issn={1225-1429},
year={2003},
volume={13},
number={3},
pages={139-144}
TY - JOUR
AU - Sang Guen Lee
AU - Eun Young Choi
AU - Lee, Yoon-bok
AU - KwangHo Kim
AU - Park,Hee-Chan
TI - Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors
JO - Journal of the Korean Crystal Growth and Crystal Technology
PY - 2003
VL - 13
IS - 3
PB - The Korea Association Of Crystal Growth, Inc.
SP - 139
EP - 144
SN - 1225-1429
AB - Nickel fine powders were prepared from nickel chloride aqueous solution containing ethanol as an organic solvent, and their oxidation behaviors were investigated. The reduction reaction by hydrazine from nickel chloride aqueous solution containing ethanol depend on reaction temperature. The reduction reaction time by hydrazine decreased with the increase of reaction temperature. By controlling reaction temperature, the products could be obtained spherical particles in the range of 0.1 μm ~1.0 μm . Also, As reaction temperature increased from 40 ∘ C to 80 ∘ C , the particle size slightly increased and had a broad size distribution owing to the presence of the coarse particles. The mean particle size and specific surface area of nickel powders prepared at 60 ∘ C were 0.3 μm and 31.8 \m 2 /g, respectively. Weight loss of the powders at 300 ∘ C was due to composition of N i(OH)2 . In case of heat treatment at 200 ∘ C in air, oxidation resistance of nickel powders was remarkable than that of as-synthesized.
KW - Nickel powder . Mixed solvent . Oxidation behavious
DO -
UR -
ER -
Sang Guen Lee, Eun Young Choi, Lee, Yoon-bok, KwangHo Kim and Park,Hee-Chan. (2003). Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors. Journal of the Korean Crystal Growth and Crystal Technology, 13(3), 139-144.
Sang Guen Lee, Eun Young Choi, Lee, Yoon-bok, KwangHo Kim and Park,Hee-Chan. 2003, "Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors", Journal of the Korean Crystal Growth and Crystal Technology, vol.13, no.3 pp.139-144.
Sang Guen Lee, Eun Young Choi, Lee, Yoon-bok, KwangHo Kim, Park,Hee-Chan "Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors" Journal of the Korean Crystal Growth and Crystal Technology 13.3 pp.139-144 (2003) : 139.
Sang Guen Lee, Eun Young Choi, Lee, Yoon-bok, KwangHo Kim, Park,Hee-Chan. Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors. 2003; 13(3), 139-144.
Sang Guen Lee, Eun Young Choi, Lee, Yoon-bok, KwangHo Kim and Park,Hee-Chan. "Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors" Journal of the Korean Crystal Growth and Crystal Technology 13, no.3 (2003) : 139-144.
Sang Guen Lee; Eun Young Choi; Lee, Yoon-bok; KwangHo Kim; Park,Hee-Chan. Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors. Journal of the Korean Crystal Growth and Crystal Technology, 13(3), 139-144.
Sang Guen Lee; Eun Young Choi; Lee, Yoon-bok; KwangHo Kim; Park,Hee-Chan. Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors. Journal of the Korean Crystal Growth and Crystal Technology. 2003; 13(3) 139-144.
Sang Guen Lee, Eun Young Choi, Lee, Yoon-bok, KwangHo Kim, Park,Hee-Chan. Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors. 2003; 13(3), 139-144.
Sang Guen Lee, Eun Young Choi, Lee, Yoon-bok, KwangHo Kim and Park,Hee-Chan. "Synthesis of nickel fine powder in the mixed solvent of water and ethanol and its oxidation behaviors" Journal of the Korean Crystal Growth and Crystal Technology 13, no.3 (2003) : 139-144.