@article{ART003089154},
author={Yong Il Park and JiHoon Jung and Sung Hyun Woo and JUNG HEON LEE and Kim Hyeong Jun},
title={Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I},
journal={Journal of the Korean Crystal Growth and Crystal Technology},
issn={1225-1429},
year={2024},
volume={34},
number={3},
pages={103-107},
doi={10.6111/JKCGCT.2024.34.3.103}
TY - JOUR
AU - Yong Il Park
AU - JiHoon Jung
AU - Sung Hyun Woo
AU - JUNG HEON LEE
AU - Kim Hyeong Jun
TI - Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I
JO - Journal of the Korean Crystal Growth and Crystal Technology
PY - 2024
VL - 34
IS - 3
PB - The Korea Association Of Crystal Growth, Inc.
SP - 103
EP - 107
SN - 1225-1429
AB - In this study, nickel, a pure metal material, was proposed as a saggar for synthesizing NCM [Li(NixCoyMnz)O₂] cathode active material. Nickel is known as a metal that is resistant to oxidation and has a high melting point. Nickel is one of the main components of NCM cathode material and was expected to be free from problems with contamination from saggar during cathode material synthesis. We sought to confirm the possibility of nickel as a saggar for synthesizing NCM cathode active materials. When a Ni metal crucible and Ni0.8Co0.1Mn0.1(OH)₂ (NCM 811) precursor material were reacted at 900°C for a long time, the change in the reaction layer on the surface of the crucible over time was analyzed. The nickel crucible reaction layer formed during heat treatment at 900°C was nickel oxide, and is thought to have been created by simultaneous oxygen diffusion from the cathode precursor oxide and reaction with oxygen in the atmosphere. The change in thickness of the oxide layer appears to slow down after 480 hours, which suggests that the rate of oxygen diffusion from the precursor is reduced. It remained combined without falling out of the crucible until 480 hours. However, it was confirmed that the oxide layer falls off after 720 hours, so it is thought that it can be used as saggar for NCM synthesis only for a certain period of time.
KW - Saggar;Nickel;Nickel oxide;NCM cathode material synthesis
DO - 10.6111/JKCGCT.2024.34.3.103
ER -
Yong Il Park, JiHoon Jung, Sung Hyun Woo, JUNG HEON LEE and Kim Hyeong Jun. (2024). Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I. Journal of the Korean Crystal Growth and Crystal Technology, 34(3), 103-107.
Yong Il Park, JiHoon Jung, Sung Hyun Woo, JUNG HEON LEE and Kim Hyeong Jun. 2024, "Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I", Journal of the Korean Crystal Growth and Crystal Technology, vol.34, no.3 pp.103-107. Available from: doi:10.6111/JKCGCT.2024.34.3.103
Yong Il Park, JiHoon Jung, Sung Hyun Woo, JUNG HEON LEE, Kim Hyeong Jun "Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I" Journal of the Korean Crystal Growth and Crystal Technology 34.3 pp.103-107 (2024) : 103.
Yong Il Park, JiHoon Jung, Sung Hyun Woo, JUNG HEON LEE, Kim Hyeong Jun. Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I. 2024; 34(3), 103-107. Available from: doi:10.6111/JKCGCT.2024.34.3.103
Yong Il Park, JiHoon Jung, Sung Hyun Woo, JUNG HEON LEE and Kim Hyeong Jun. "Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I" Journal of the Korean Crystal Growth and Crystal Technology 34, no.3 (2024) : 103-107.doi: 10.6111/JKCGCT.2024.34.3.103
Yong Il Park; JiHoon Jung; Sung Hyun Woo; JUNG HEON LEE; Kim Hyeong Jun. Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I. Journal of the Korean Crystal Growth and Crystal Technology, 34(3), 103-107. doi: 10.6111/JKCGCT.2024.34.3.103
Yong Il Park; JiHoon Jung; Sung Hyun Woo; JUNG HEON LEE; Kim Hyeong Jun. Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I. Journal of the Korean Crystal Growth and Crystal Technology. 2024; 34(3) 103-107. doi: 10.6111/JKCGCT.2024.34.3.103
Yong Il Park, JiHoon Jung, Sung Hyun Woo, JUNG HEON LEE, Kim Hyeong Jun. Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I. 2024; 34(3), 103-107. Available from: doi:10.6111/JKCGCT.2024.34.3.103
Yong Il Park, JiHoon Jung, Sung Hyun Woo, JUNG HEON LEE and Kim Hyeong Jun. "Study on the feasibility of metallic saggar for synthesizing NCM cathode active materials-I" Journal of the Korean Crystal Growth and Crystal Technology 34, no.3 (2024) : 103-107.doi: 10.6111/JKCGCT.2024.34.3.103
