Effect of ethylene glycol on the nano-sized ZnO nanoparticles using polyol process (폴리올 공정을 이용한 에틸렌 글리콜이 나노 크기의 산화아연 나노입자에 미치는 영향)

Dae-Hwan Jang (장대환); Bo-Ram Kim (김보람); Kim Dae Weon (김대원)

doi:10.6111/JKCGCT.2024.34.4.117

Effect of ethylene glycol on the nano-sized ZnO nanoparticles using polyol process

Journal of the Korean Crystal Growth and Crystal Technology
Abbr : J. Korean Cryst. Growth Cryst. Technol.
2024, 34(4), pp.117~124
DOI : 10.6111/JKCGCT.2024.34.4.117
Publisher : The Korea Association Of Crystal Growth, Inc.
Research Area : Engineering > Materials Science and Engineering
Received : July 1, 2024
Accepted : July 18, 2024
Published : August 31, 2024

Dae-Hwan Jang ¹, Bo-Ram Kim ², Kim Dae Weon ³

¹고등기술연구원
²삼성 SDI 리사이클연구소
³고등기술연구원연구조합

Accredited

ABSTRACT

Zinc oxide nanoparticles were synthesized using the polyol method with ethylene glycol containing hydroxyl groups (-OH). It was confirmed that the zinc compounds prepared by the polyol method were a mixture of zinc carbonatehydroxide (Zn₅(OH)₆(CO₃)₂) and zinc oxide (ZnO) crystalline structures. Calcination at 400°C, 600°C and 800°C was performed to examine the effects of calcination temperature on the particle size, morphology and crystallinity of zinc oxide. ZnO powders of calcination at 800°C was evaluated to particle size analysis from ethylene glycol containing precursor solution compared with distilled water based solution. The zinc oxide particles obtained from the former had a particle size of approximately 404 ± 51 nm, whereas those from the latter exhibited a more uniform nanoparticles morphology with aparticle size of approximately 109 ± 29 nm. This demonstrates that the addition of ethylene glycol can control the influence of water molecules, enabling the direct synthesis of zinc oxide in the form of uniform nanoparticles.

KEYWORDS

Zinc oxide, Nanoparticles, Ethylene glycol, Polyol, Particle size

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Journal of the Korean Crystal Growth and Crystal Technology 2025 KCI Impact Factor : 0.14 KCI-WoS Impact Factor : 0.45

Effect of ethylene glycol on the nano-sized ZnO nanoparticles using polyol process

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* References for papers published after 2025 are currently being built.

Journal of the Korean Crystal Growth and Crystal Technology 2025 KCI Impact Factor : 0.14 KCI-WoS Impact Factor : 0.45

Effect of ethylene glycol on the nano-sized ZnO nanoparticles using polyol process

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